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philip > General Lab Stuff > Flashcards

General Lab Stuff Flashcards

1
Q

When prepping solutions pay attention to all that you add why?

A

Expiration date

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2
Q

Dryers all dries except are on

A

Except the 5 are on the east side

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3
Q

gabe uplc wash station where is it

A

-

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4
Q

CPH

A

codeine phospahte

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5
Q

You keep doing it! Exp date

A

7/2017 6/2018 instruments

Whole exp for reagents

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6
Q

Michelle eye contact empower

A

Look at bottom for processing method

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7
Q

When prepping standards remember to write what down Cristina

And to always look at the

A

Standard number E number and NQS nnumebr

COA

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8
Q

you may find what about the reactors inside the sample

A

the lining

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9
Q

Receiving chemicals EC procedure

A
  • intelletrack __receive__ location chemical intentory __ scan sample__ write exp date in the batch
  • check binder for COA___ if not google and highlight exp and batch number___ D/I
  • scan it __put it in L drive: - swedes – department shared

– quality services – chemical CofAs
You find the scan in applications helpful links Xerox swedes

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10
Q

Justin expression snug is

A

Great

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11
Q

Michelle Steve npma la training how to find KF values for old batches in SAP

A

QE13 or QA13, delete inspection points
Mark all the checks on the left, put 1/1/16 on created and enter batch number in the bottom.

Use the new inspection number to search for the info .

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12
Q

nPOB2 fro sg becomes —— npob2 becomes

A

POBSG ——- nOXY wet, nOXY dry now it follows the same as

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13
Q

NR samples don’t get

A

SAP

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14
Q

When DEA is reported in SAP remember to write it down in

A

The logbook

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15
Q

When receiving into intellitrack always check if the material is non controlled or controlled.

A

All non controlled are immediately disposed of.

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16
Q

Michelle mistake reprocessing

A

All peaks have to be labeled in impurities run

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17
Q

for expirations dates of MPs and diluents see

A

Test procedures

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18
Q

OMH

A

Oxymorphone hydrochloride

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19
Q

Zach palladium in ML are —– with what

A

deactivated with sodium bisulfite

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20
Q

What to take with you when throwing waste out

A

Key secondary container mask start accumulation date labels

There is also a container for needles ?

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21
Q

to determine w standard conc

A

multiply the conc from the sol or stock by the DF

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22
Q

agilent vs waters system that draws sampole

A

metering piston sample syringe

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23
Q

expiration date from opened for pH buffers

A

30 days

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24
Q

how are products classified according to mill passes

A

fine x fine and micronized

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25
Q

Remember COP what (you get asked this a lot)

A

Location building or whatever

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26
Q

if you circled yes for indefinitely stable

A

make sure to finishing filling th e sicker when it is opened

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27
Q

HBT

A

Hydrocodone bitartrate

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28
Q

terms to remeber gabe uplc

A

needle wash syringe, sample loop, sample manager, low needle, sample prsh

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29
Q

AMA

A

Morphine base

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30
Q

nPOB reaction train

A

nPOB 2 wet splits into nPOB2 for POB for sg and nPOB-2

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31
Q

When logging in swabs first do

A

IT first comments go description

Then sit in your office and do SAP

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32
Q

ACA

A

anhydrous codeine alkaloid

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33
Q

SIL

A

Sample in lab

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34
Q

tapentadol train reaction

A

T2955 T3014 T3028 Wet T3028 Dry

35
Q

Dilution factor= ?

A

= solute/total colume

10/50 = 0.2

36
Q

What is the bill of lading?

A

Check MFG and disctributor adress this is used to determined reduced or full testing

Make sure its legible

37
Q

remember how to access

A

MSDS hazardous waste spreadsheet

38
Q

According to gabe, A and B mobile pahses are usually what

A

A aqueous

B is organic

39
Q

what direction to loosen helium tanks

A

down

40
Q

POB 3 wet reaction train

A

POB 3 wet -> POB 3 dry ->OXY 3 wet -> Oxy3 dry -> splits into oxy3 course oxy 3 first mill pass and oxy 3 STD

41
Q

ss suit is good until the time of the

A

last injection

42
Q

NPMa Steve second shift assay prep

A

Use the Tare button to get an idea

the weight of the weigh boats can vary

Go as low as possible for assay and as high as possible for impurities

43
Q

oxy train reaction

A

CPS thebaine -> nCOB -> splits into POB3 wet and nPOB

44
Q

AMP and Tap DEA detail

A

they have separate DEA sample preparation procedure

45
Q

remember the zach UPLC technique he was teaching jakie

A

reset SM or whatever

46
Q

Remember Brett change procedure column

A

Clips in the union

Circle around to the magnet

47
Q

Documents to check when receing tankers and what to check on them

A

-COA
-BO Lading
-Wash Certificate must be signed (Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter
Check that they are initial and date and batch from someone from the warehouse

48
Q

If your NIR residuals are out what to do?

A

Go to your primary method.

49
Q

what is a destruction form ?

A

it destroys a current analytical worksheet and replaces it with another one

50
Q

Coa STD

A

Purity factor
Dried?
Ref std/Enumbrr
Retest date

51
Q

when writing up Working standards in the SLN log book do not forget to

A

write the conc and the units

52
Q

freezer safe password

A

11*1111#

53
Q

how to fix the pan balances rachel leveling

A

unlock the hooks in the back turn the wheels in the front

54
Q

Before acquiring gross weights remember what about the stickers

A

add all stickers because they add weight

55
Q

COP that require swabs first need to be —- before going —-

A

Reviewed swabbing

56
Q

oxy 3 first mill pass splits into

A

oxy 3 fine, x fine and micronized

57
Q

Did I turn it off? I’m so stupid

A

GC Michhelle

58
Q

Do not forget the timer when doing

A

LOD

59
Q

Start using more —- mistake Christina HCB

A

Timer

60
Q

When being the first in the lab

A

Remember to do the balances and check the 5s thing

61
Q

OMH final retains go in

A

The fridge

62
Q

Methanol / water bubbles

A

Stir really good

63
Q

dont forget new tricks NP SAP

A

deselect all, new selection

64
Q

transcation to look up older results in SAP

A

QA13

hit the thing to the side enter batch use that inspection number

65
Q

how to look up who did something in SAP jaitin sarak

A

select do the calendar thing and look up in browse JJEDS employee green

66
Q

empower names for the things you do to the side

A

transaction codes we use QE51N

67
Q

what do you do in special cases when fro exam[ple SAP ask you for a certain number of digits and it fails a sample?

A

you force close it in SAP

68
Q

SAP <0.05 mistake fix

A

jatin look to the right the arrow menu

69
Q

Communication category clean out swabs

A

Clean out swabs and tucker communication

70
Q

End of month cycle category

A

Ph frita vwds

71
Q

OMH Finals uv vis Jatin kool aid man

A

Uv VI’s you hit ok instead of finish

72
Q

Gave fridge tucker 9 things you will explain that to me right? Location of Nishma

A

Temperature mapping of chart recorder

73
Q

On the LC 1200 at the end of the month the 2 things that get changed are

A

The Frits and the column guard

74
Q

Mentally review column guard and grit change

A

–tucker

75
Q

VWD test

A 
Get water 
Take out column 
Put in straight line 
Open purge 5 for 5 min 
Close 1.5 flow 
Lamp test
76
Q

Swab details volume of what

A

25 mililitros of 1.5 phosphoric
1 dry one wet
Don’t forget the ammonium hydroxide

77
Q

Always remembering what when doing anything in the works sheet

A

Always signed a performed by

78
Q

If you want the oven temp to go lower

A

Leave the open door

79
Q

If you want to reduce the chance of something being out of the oven affecting you

A

Put it ina. Dessiqctr

80
Q

When trouble shooting impurities in mobile phase remember to

A

Filter

81
Q

GC Change syringe don’t forget the

A

Flap

82
Q

Get into the habit of writing the exp date last why?

A

Wait until you add everything the last thing on there is your exp date

83
Q

How to make your retains faster?

A
  • after your done immediately go to the IT balance to confirm final weight
  • ## don’t double check net weight calculation IT will do it for you

philip (20 decks)

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