Chemical Analysis Flashcards

(31 cards)

1
Q

What is a pure substance in chemistry

A

A substance is a single element or compound that is not mixed with any other substance

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2
Q

What is a pure substance in everyday language

A

A substance that has had nothing added to it

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3
Q

What is a formulation

A

A mixture that has been designed as a useful product, with carefully measured components so the product has desired and required properties.

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4
Q

What does Paper Chromatography do

A

Separates the different dyes in an ink

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5
Q

Describe paper chromatography method (7 steps)

A

1- take filter paper and draw line in pencil near bottom (base line)
2 - add sample of ink to baseline
3 - Fill beaker with shallow amount of solvent
4 - Place filter paper into solvent
5 - Don’t submerge ink in solvent
6 - Place lid on top of beaker to stop the solvent evaporating
7 - Wait for solvent to seep up paper, dyes will dissolve in solvent and move up with it at different rates
8 - Take paper out and leave to dry

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6
Q

What happens to un soluble substances in paper chromatography

A

Stay on the base line

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7
Q

What is the mobile phase

A

Substance the molecules can move in (solvent)

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8
Q

What is the stationary phase

A

Substance the molecules can’t move in (paper)

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9
Q

Why do more soluble substances move up further

A

Spend more time in the mobile phase, so move faster
Less soluble are more attracted to the paper and spend more time in the stationary phase

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10
Q

How to calculate Rf value

A

Distance travelled by substane / distance travelled by solvent

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11
Q

Test for hydrogen

A
  • Burning splint held at the open end of a test tube of the gas
  • Hydrogen burns rapidly with a pop sound
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12
Q

Test for oxygen

A
  • Glowing splint inserted into a test tube of the gas
  • The splint relights in oxygen
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13
Q

Test for carbon dioxide

A
  • Use aqueous solution of limewater, will turn cloudy when co2 is bubbled through it
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14
Q

Test for chlorine

A
  • Damp litmus paper bleaches and turns white in presence of chlorine gas
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15
Q

What do lithium compounds result in during flame test

A

Crimson flame

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16
Q

What do sodium compounds result in during flame test

17
Q

What do potassium compounds result in during flame test

18
Q

What do calcium compounds result in during flame test

A

Orange/red flame

19
Q

What do copper compounds result in during flame test

20
Q

What solutions form white precipitate and when

A

When sodium hydroxide solution is added,
Aluminium
Calcium
Magnesium
But magnesium hydroxide precipitate dissolves in excess sodium hydroxide solution

21
Q

When sodium hydroxide is added, what colour precipitate does copper (ii) form

22
Q

When sodium hydroxide is added, what colour precipitate does iron (ii) form

23
Q

When sodium hydroxide is added, what colour precipitate does iron(iii) form

24
Q

Test for carbonates

A

Will react with dilute acids to form co2, which can be identified using limewater

25
Test for halides
Produces precipitates with silver nitrate, if in the presence of dilute nitric acid
26
What colour precipitate is silver chloride
White
27
What colour precipitate is silver bromide
Cream
28
What colour precipitate is silver iodide
Yellow
29
Test for sulphates
Produce a white precipitate with barium chloride solution in the presence of HCL
30
Give an example of an instrumental method of analysing elements and compounds
Flame emission spectroscopy
31
Explain briefly how to carry out flame emission spectroscopy
Place sample into a flame and the light given out is passed through a spectroscope. The output is a line spectrum that can be analysed to identify metal ions and their concentration