chemical analysis Flashcards

(34 cards)

1
Q

What is a pure substance ?

A

-a single element or compound, not mixed with any other substance.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
2
Q

How can you distinguish pure substances from mixtures?

A
  • Pure substances have specific melting and boiling points while mixtures melt and boil over a range of temperatures
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
3
Q

what is a pure substance in everyday?

A

-a substance that has had nothing added to it, so it is unadulterated and in its natural state, eg pure milk.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
4
Q

What is a formulation and how is it made?

A

-a mixture designed as a useful product, made by mixing chemicals in carefully measured quantities to ensure the product has specific properties.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
5
Q

Can you name some examples of formulations?

A

-fuels, cleaning agents, paints, medicines, alloys, fertilizers, and foods.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
6
Q

What is chromatography used for?

A
  • to separate mixtures and it can help identify substances based on how they move between a stationary and mobile phase.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
7
Q

What is the formula for Rf value?

A
  • Rf = (Distance moved by substance) / (Distance moved by solvent)
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
8
Q

How can Rf values help identify compounds?

A
  • Different compounds have different Rf values in various solvents, which can help identify them. A pure compound will always produce a single spot in all solvents.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
9
Q

How do you test for hydrogen gas?

A

-Hydrogen burns rapidly with a pop sound when a burning splint is held at the open end of a test tube containing the gas.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
10
Q

How do you test for oxygen gas?

A
  • Oxygen will relight a glowing splint when it is inserted into a test tube of the gas.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
11
Q

How do you test for carbon dioxide gas?

A
  • Carbon dioxide turns limewater cloudy when it is bubbled through or shaken with an aqueous solution of calcium hydroxide.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
12
Q

How do you test for chlorine gas?

A
  • Chlorine bleaches and turns litmus paper white when damp litmus paper is exposed to the gas.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
13
Q

What flame color does lithium produce in a flame test?

A
  • Lithium produces a crimson flame.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
14
Q

What flame color does sodium produce in a flame test?

A
  • Sodium produces a yellow flame.
How well did you know this?
1
Not at all
2
3
4
5
Perfectly
15
Q

What flame color does potassium produce in a flame test?

A

-Potassium produces a lilac flame.

How well did you know this?
1
Not at all
2
3
4
5
Perfectly
16
Q

What flame color does calcium produce in a flame test?

A

-Calcium produces an orange-red flame.

17
Q

What flame color does copper produce in a flame test?

A

-Copper produces a green flame.

18
Q

How do sodium hydroxide tests help identify metal ions?

A
  • Some metal ions form precipitates with sodium hydroxide. For example, aluminium, calcium, and magnesium form white precipitates, while copper(II), iron(II), and iron(III) form coloured precipitates.
19
Q

What happens when aluminium hydroxide is added to excess sodium hydroxide?

A
  • Aluminium hydroxide dissolves in excess sodium hydroxide.
20
Q

What colors do copper(II), iron(II), and iron(III) precipitates form with sodium hydroxide?

A
  • Copper(II) forms a blue precipitate, iron(II) forms a green precipitate, and iron(III) forms a brown precipitate.
21
Q

What reaction occurs when carbonates react with dilute acids?

A

-Carbonates react with dilute acids to produce carbon dioxide gas, which can be identified by turning limewater milky.

22
Q

What do halide ions form when reacted with silver nitrate solution?

A

-: Halide ions form precipitates with silver nitrate in the presence of dilute nitric acid: silver chloride is white, silver bromide is cream, and silver iodide is yellow.

23
Q

What happens when sulfate ions react with barium chloride solution?

A

-Sulfate ions produce a white precipitate with barium chloride in the presence of dilute hydrochloric acid.

24
Q

What is flame emission spectroscopy used for?

A

-to analyze metal ions in solutions by observing the light emitted by the sample when it is placed in a flame.

25
How does flame emission spectroscopy work?
- The sample is placed in a flame, and the light emitted is passed through a spectroscope. The resulting line spectrum can identify the metal ions and measure their concentration.
26
describe the required practical for paper chromatography
* first we draw a starting line on the chromatography paper using a pencil * place spot of food colouring on start line * place solvent in beaker * place chromatography paper in beaker * so chromatography paper is in solvent * make sure solvent is below start line * use a lid * wait for solvent to travel up the chromatography paper until close to top * mark solvent front * dry the chromatography paper * measure distance between start line and centre of spot * measure distance between start line and solvent front -use these measurements to calculate Rf value
27
what is the stationary phase?
-the paper because it does not move
28
what is the mobile phase?
-the solvent as it does move
29
why do we draw our starting line in pencil?
-if we drew the line in pen, the pen ink would move up the paper, with the solvent
30
why might we need to repeat the experiment using a different solvent?
-several different substances could have the same Rf value
31
what happens if the substance has never been analysed before?
-there will not be an Rf value on the database so further investigation needs to be carried out
32
what are disadvantages of flame tests?
-the colour of a flame test can be difficult to distinguish especially if there is only a low concentration of the metal compound -sometimes a sample contains a mixture of metal ions which can mask the colour of the flame
33
what is flame emission spectroscopy an example of?
-an instrumental method
34
state the three advantages of flame emission spectroscopy
-instrumental methods are rapid as flame emission spectroscopy analyses samples more rapidly than flame tests -instrumental methods are sensitive - flame emission spectroscopy will work even on a tiny sample of metal compound -instrumental methods are accurate.Flame emission spectroscopy is more likely to identify a metal ion correctly than using a flame test