chemical analysis Flashcards

(30 cards)

1
Q

what is a pure substance?

A

a substance which contains only one type of compound or element e.g. pure water

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2
Q

give a property of pure substances

A

they melt and boil at specific temperatures

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3
Q

how do impure substances melt and boil?

A

impure substances melt and boil over a range of temperatures depending on how much of each substance is in the mixture

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4
Q

having impurities in substances will generally…

A

lower the melting point but increase the boiling point

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5
Q

what is a formulation?

A

a formulation is a mixture with a specific composition for a specific application/need

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6
Q

give 3 examples of formulations

A

-fuels
-medicines
-alloys

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7
Q

what is an element?

A

a substance made up of only type of atom

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8
Q

what is a mixture?

A

two or more different elements that are not chemically bonded

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9
Q

what is a compound?

A

a substance made up of two or more different types of elements that are chemically bonded

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10
Q

define chromatography

A

chromatography is a separation technique that separates mixtures with different rf values

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11
Q

give the first 3 steps for a paper chromatography method?

A

1-take a piece of filter paper and use a pencil to draw a line 3cm from the bottom of the sheet
2-add your substances of ink onto the pencil line using a pipette
3-fill a beaker with a shallow amount of water or ethanol, this is your solvent

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12
Q

give steps 4-5 for paper chromatogram method

A

4-place the filter paper into the solvent ensuring you do not submerge your pencil line and ink and secure the paper to a pencil using paper clips-rest on beaker (so it doesn’t fall)
5-place a lid on top to stop the solvent from evaporating

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13
Q

give steps 6-7 for the paper chromatogram method

A

6-allow the solvent to move through the paper, but remove the chromatogram before it reaches the top
7-allow the chromatogram to dry, then measure the distance travelled by each spot and by the solvent from the baseline

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14
Q

what is the stationary phase?

A

a substance or material that the molecules cannot move in-eg the paper

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15
Q

what is the mobile phase?

A

a substance that the molecules can move in-always a liquid or gas-eg the solvent

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16
Q

give the equation to calculate a rf value

A

distance substance moved/distance solvent moved

17
Q

how do we test for chlorine?

A

to test for chlorine we insert damp litmus paper into the mouth of the test tube

18
Q

what is the positive result for a chlorine test?

A

the chlorine will decolourise the litmus paper and turn it white

19
Q

how do we test for hydrogen?

A

to test for hydrogen we remove the bung and insert a burning splint into the test tube “squeaky pop test”

20
Q

what is the positive result for a hydrogen test?

A

hydrogen gas burns rapidly-produces a pop sound

21
Q

how do we test for oxygen?

A

use a glowing splint and place into the test tube

22
Q

what is the positive result for a oxygen test?

A

the splint will relight

23
Q

how do we test for co2?

A

to test for co2 we use limewater-draw some of the gas into a pipette and bubble the gas through the limewater, and repeat

24
Q

what is the positive result for a co2 test?

A

if co2 is present the limewater will turn cloudy

25
how do we test for ammonia?
place a piece of blue litmus paper into the test tube
26
what is the positive result for an ammonia test?
the blue litmus paper will turn red
27
what is the formula for ammonia?
NH3
28
why do the substances in the mixtures of ink separate in the mobile phase?
the substances will have different solubilities making some travel further than others on the chromatogram
29
how can impurities affect the melting and boiling points of the sample?
-lower the melting point -increase the boiling point -increase the range over which substances melt and boil
30
what physical test can you do to check that a substance is pure?
heat it until it melts and boils-if it melts or boils at a specific temperature then it is pure(rather than over a range of temperatures)