practicals Flashcards
Describe the titration practical
1) Use a pipette to tansfer 25cmcubed of sodium hydroxide solution into a conical flask
2) add 5 drops of an indicator to the alkali in the flask
3) Use a white tile under the conical flask to see a colour change more clearly
4) Fill a burrete with sulfuric acid
5) add acid to the alkali until the solution is neutral once a colour change is seen add the acid drop by drop until the solution is neutral. It is importsnt to swirl the solution to make sure the acid and alkali mix
6)Read the volume of acid in the burette
What to do to make the experiment more accurate
Mix/swirl the flask while acid is poured
repeat experiment and calculate a mean
when reading the burette, ignore bubbles
What is the titration formula
sulfuric acid + sodium hydroxide -> sodium sulfate + water
Why can’t solid ionic compounds conduct electricity
the ions are locked in place and are not free to move
strong electrostatic forces of attraction
In electrolysis how do we use ionic compounds
It is melted or dissolved in water, this breaks the forces of attraction and the ions are free to move
These liquids can now conduct electricity
scientists call these liquids electrolytes
cathode
negative electrode
anode
positive electrode
What happens at the anode and cathode
At the anode, the negative ions are attracted to the anode and loose electrons to become oxidised as they loose electrons
At the cathode the positive ions are attracted and gain electrons, becoming reduced
What is produced at the cathode if the metal is more reactive than hydrogen
hydrogen
(copper and silver are less reactive)
what is produced at the anode
oxygen
What is used as an electrode and why
platnum is used as it is inert
Graphite, made out of carbon and a good conductor of electricity and a high melting point
How do we electrolyse aluminium oxide
1) aluminium oxide has a high melting point so first it’s mixed with cryolite which lowers the melting point
2)Then we apply an electric current to the aluminium oxide
3) Al3+ is attracted to cathode, gains electrons and forms aluminium atom (reduction)
4) O2- are attracted to anode, (oxidised)
Why do we use cryolite
reduces the amount of energy needed to melt aluminium oxide and so it saves money
What’s wrong with electrolysis
The anode must be replaced regularly because the oxgygen produced at the anode react with the graphite(carbon) to form carbon dioxide gas.
a lot of energy is required to produce an electric current