C12 - Testing substances Flashcards

1
Q

test for hydrogen = positive

A

lighted splint pops

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2
Q

test for o2 = positive

A

a glowing splint relights

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3
Q

test fro co2

A

turns limewater milky

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4
Q

test for chlorine

A

damp blue litmus paper turns white (bleaches)

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5
Q

flame tests process

A

-nichrome wire loop dipped into concentrated HCL to clean it
-dipped into HCL + metal compound
-hold loop in blue bunsen burner flame
-colour = identifies metal ion

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6
Q

flame tests

A

identifies metal ion by colour of flame

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7
Q

mixture of metal ions in flame test

A

colours can be masked

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8
Q

Li+ flame colour

A

crimson

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9
Q

Na+ flame colour

A

yellow

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10
Q

K+ flame colour

A

lilac

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11
Q

flame colour of Ca2+

A

orange - red

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12
Q

Cu2+ flame colour

A

green

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13
Q

Mg2+ flame colour

A

no colour

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14
Q

metal cation test is with

A

sodium hydroxide

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15
Q

metal cation test with sodium hydroxide test

A

identifies metal positive ions in unknown compound

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16
Q

metal cation test with sodium hydroxide for aluminium, calcium, magnesium

A

white precipitate

17
Q

metal cation test with sodium hydroxide - aluminium

A

precipitate will dissolve

18
Q

metal cation test with sodium hydroxide test - mg and ca

A

precipitate will not dissolve
-then can be distinguished with a flame test

19
Q

copper II ions colour precipitate

20
Q

iron II ions colour precipitate

21
Q

iron III ions colour precipitate

22
Q

testing for carbonate

A

fizzing + co2 produced
-when dilute acid is dded

23
Q

group 1 carbonates

A

soluble whereas most aren’t

24
Q

Halide test

A

add dilute nitric acid and silver nitrate solution
-if a precipitate forms = present

25
halide test - why add nitric acid
-to dissolve compound and remove carbonate ions -prevents a precipitate forming with silver ions + carbonate and interfere with the test
26
halide colour precipitate
I = yellow Cl = white Br = cream
27
sulfate test
-add dilute HCL and barium chloride solution
28
sulfate test - why add HCL
removes carbonate ions to precipitatae doesn't form with barium ions
29
sulfate test present
-white precipitate -this is insoluble barium sulfate
30
modern instrumental pros
-highly accurate -sensitive -quicker -allow small samples to be analysed
31
cons of modern instruments
-expensive -special training -only interpreted by comparing to known substances
32
flame emission spectroscopy
-analyse samples for metal ions
33
flame emission spectroscopy process
-sample is heated in a flame -energy provided excites electrons in metal ions -allows them o jump to higher energy levels -when they fall back to lower levels = energy is released as light
34
spectrometer
wavelengths of light produced can be analysed by passing through this
35
spectrometer - metal ions
-each type absorbs/emits its own line spectrum
36
line spectrum
own characteristic pattern of radiation -identifies metal ions by comparing to a database on a computer
37
spectrometer on concentration
-measures intensity of light with a specific wavelength of a particular metal ion -machine is calibrated sing known concentrations to give a value
38
spectrometer pros
-provide accurate ways to monitor water for metal ions
39
spectrometer used in
steel industry -controls trace metals present = quality