C16- Organic synthesis Flashcards
(13 cards)
Alkane to bromoalkane
Uv light
Br2
Alkene to alkane
H2
Nickel catalyst
Alkene to dibromoalkane
Bromine
RTP
(bromine water pretty much)
Electrophilic addition
Bromoalkane to alcohol
NaOH
Reflux
Nucleophilic substitution
Secondary alcohol to ketone
Reflux
K2Cr2O7 / H2SO4
Primary alcohol to bromoalkane
NaBr
H2SO4
Reflux
Alkene to bromoalkane
Hbr
RTP
Primary alcohol to alkene
Conc H2SO4
Reflux
Alkene to alcohol
H2O
300c
Acid catalyst (H3PO4)
Primary alcohol to aldehyde
Distil of product
K2Cr2O7 / H2SO4
Aldehyde to carboxylic acid
Reflux
K2Cr2O7 / H2SO4
4 key steps to purification of an organic product
Separating funnel
Neutralise leftover acid catalyst
Anhydrous salt
Resdistil and measure bp
Why add sodium carbonate to purify an organic product
neutralises acid