General Lab Stuff

Question 1

When prepping solutions pay attention to all that you add why?

Answer 1

Expiration date

Question 2

Dryers all dries except are on

Answer 2

Except the 5 are on the east side

Question 3

gabe uplc wash station where is it

Answer 3

-

Question 4

CPH

Answer 4

codeine phospahte

Question 5

You keep doing it! Exp date

Answer 5

7/2017 6/2018 instruments

Whole exp for reagents

Question 6

Michelle eye contact empower

Answer 6

Look at bottom for processing method

Question 7

When prepping standards remember to write what down Cristina

And to always look at the

Answer 7

Standard number E number and NQS nnumebr

COA

Question 8

you may find what about the reactors inside the sample

Answer 8

the lining

Question 9

Receiving chemicals EC procedure

Answer 9

• intelletrack __receive__ location chemical intentory __ scan sample__ write exp date in the batch
• check binder for COA___ if not google and highlight exp and batch number___ D/I
• scan it __put it in L drive: - swedes – department shared

– quality services – chemical CofAs
You find the scan in applications helpful links Xerox swedes

Question 10

Justin expression snug is

Answer 10

Great

Question 11

Michelle Steve npma la training how to find KF values for old batches in SAP

Answer 11

QE13 or QA13, delete inspection points
Mark all the checks on the left, put 1/1/16 on created and enter batch number in the bottom.

Use the new inspection number to search for the info .

Question 12

nPOB2 fro sg becomes —— npob2 becomes

Answer 12

POBSG ——- nOXY wet, nOXY dry now it follows the same as

Question 13

NR samples don’t get

Answer 13

SAP

Question 14

When DEA is reported in SAP remember to write it down in

Answer 14

The logbook

Question 15

When receiving into intellitrack always check if the material is non controlled or controlled.

Answer 15

All non controlled are immediately disposed of.

Question 16

Michelle mistake reprocessing

Answer 16

All peaks have to be labeled in impurities run

Question 17

for expirations dates of MPs and diluents see

Answer 17

Test procedures

Question 18

OMH

Answer 18

Oxymorphone hydrochloride

Question 19

Zach palladium in ML are —– with what

Answer 19

deactivated with sodium bisulfite

Question 20

What to take with you when throwing waste out

Answer 20

Key secondary container mask start accumulation date labels

There is also a container for needles ?

Question 21

to determine w standard conc

Answer 21

multiply the conc from the sol or stock by the DF

Question 22

agilent vs waters system that draws sampole

Answer 22

metering piston sample syringe

Question 23

expiration date from opened for pH buffers

Answer 23

30 days

Question 24

how are products classified according to mill passes

Answer 24

fine x fine and micronized

Question 25

Remember COP what (you get asked this a lot)

Answer 25

Location building or whatever

Question 26

if you circled yes for indefinitely stable

Answer 26

make sure to finishing filling th e sicker when it is opened

Question 27

HBT

Answer 27

Hydrocodone bitartrate

Question 28

terms to remeber gabe uplc

Answer 28

needle wash syringe, sample loop, sample manager, low needle, sample prsh

Question 29

AMA

Answer 29

Morphine base

Question 30

nPOB reaction train

Answer 30

nPOB 2 wet splits into nPOB2 for POB for sg and nPOB-2

Question 31

When logging in swabs first do

Answer 31

IT first comments go description | Then sit in your office and do SAP

Question 32

ACA

Answer 32

anhydrous codeine alkaloid

Question 33

SIL

Answer 33

Sample in lab

Question 34

tapentadol train reaction

Answer 34

T2955 T3014 T3028 Wet T3028 Dry

Question 35

Dilution factor= ?

Answer 35

= solute/total colume | 10/50 = 0.2

Question 36

What is the bill of lading?

Answer 36

Check MFG and disctributor adress this is used to determined reduced or full testing Make sure its legible

Question 37

remember how to access

Answer 37

MSDS hazardous waste spreadsheet

Question 38

According to gabe, A and B mobile pahses are usually what

Answer 38

A aqueous | B is organic

Question 39

what direction to loosen helium tanks

Answer 39

down

Question 40

POB 3 wet reaction train

Answer 40

POB 3 wet -> POB 3 dry ->OXY 3 wet -> Oxy3 dry -> splits into oxy3 course oxy 3 first mill pass and oxy 3 STD

Question 41

ss suit is good until the time of the

Answer 41

last injection

Question 42

NPMa Steve second shift assay prep

Answer 42

Use the Tare button to get an idea the weight of the weigh boats can vary Go as low as possible for assay and as high as possible for impurities

Question 43

oxy train reaction

Answer 43

CPS thebaine -> nCOB -> splits into POB3 wet and nPOB

Question 44

AMP and Tap DEA detail

Answer 44

they have separate DEA sample preparation procedure

Question 45

remember the zach UPLC technique he was teaching jakie

Answer 45

reset SM or whatever

Question 46

Remember Brett change procedure column

Answer 46

Clips in the union Circle around to the magnet

Question 47

Documents to check when receing tankers and what to check on them

Answer 47

-COA -BO Lading -Wash Certificate must be signed (Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter Check that they are initial and date and batch from someone from the warehouse

Question 48

If your NIR residuals are out what to do?

Answer 48

Go to your primary method.

Question 49

what is a destruction form ?

Answer 49

it destroys a current analytical worksheet and replaces it with another one

Question 50

Coa STD

Answer 50

Purity factor Dried? Ref std/Enumbrr Retest date

Question 51

when writing up Working standards in the SLN log book do not forget to

Answer 51

write the conc and the units

Question 52

freezer safe password

Answer 52

11*1111#

Question 53

how to fix the pan balances rachel leveling

Answer 53

unlock the hooks in the back turn the wheels in the front

Question 54

Before acquiring gross weights remember what about the stickers

Answer 54

add all stickers because they add weight

Question 55

COP that require swabs first need to be ---- before going ----

Answer 55

Reviewed swabbing

Question 56

oxy 3 first mill pass splits into

Answer 56

oxy 3 fine, x fine and micronized

Question 57

Did I turn it off? I'm so stupid

Answer 57

GC Michhelle

Question 58

Do not forget the timer when doing

Answer 58

LOD

Question 59

Start using more ---- mistake Christina HCB

Answer 59

Timer

Question 60

When being the first in the lab

Answer 60

Remember to do the balances and check the 5s thing

Question 61

OMH final retains go in

Answer 61

The fridge

Question 62

Methanol / water bubbles

Answer 62

Stir really good

Question 63

dont forget new tricks NP SAP

Answer 63

deselect all, new selection

Question 64

transcation to look up older results in SAP

Answer 64

QA13 hit the thing to the side enter batch use that inspection number

Question 65

how to look up who did something in SAP jaitin sarak

Answer 65

select do the calendar thing and look up in browse JJEDS employee green

Question 66

empower names for the things you do to the side

Answer 66

transaction codes we use QE51N

Question 67

what do you do in special cases when fro exam[ple SAP ask you for a certain number of digits and it fails a sample?

Answer 67

you force close it in SAP

Question 68

SAP <0.05 mistake fix

Answer 68

jatin look to the right the arrow menu

Question 69

Communication category clean out swabs

Answer 69

Clean out swabs and tucker communication

Question 70

End of month cycle category

Answer 70

Ph frita vwds

Question 71

OMH Finals uv vis Jatin kool aid man

Answer 71

Uv VI's you hit ok instead of finish

Question 72

Gave fridge tucker 9 things you will explain that to me right? Location of Nishma

Answer 72

Temperature mapping of chart recorder

Question 73

On the LC 1200 at the end of the month the 2 things that get changed are

Answer 73

The Frits and the column guard

Question 74

Mentally review column guard and grit change

Answer 74

--tucker

Question 75

VWD test

Answer 75

``` Get water Take out column Put in straight line Open purge 5 for 5 min Close 1.5 flow Lamp test ```

Question 76

Swab details volume of what

Answer 76

25 mililitros of 1.5 phosphoric 1 dry one wet Don't forget the ammonium hydroxide

Question 77

Always remembering what when doing anything in the works sheet

Answer 77

Always signed a performed by

Question 78

If you want the oven temp to go lower

Answer 78

Leave the open door

Question 79

If you want to reduce the chance of something being out of the oven affecting you

Answer 79

Put it ina. Dessiqctr

Question 80

When trouble shooting impurities in mobile phase remember to

Answer 80

Filter

Question 81

GC Change syringe don't forget the

Answer 81

Flap

Question 82

Get into the habit of writing the exp date last why?

Answer 82

Wait until you add everything the last thing on there is your exp date

Question 83

How to make your retains faster?

Answer 83

- after your done immediately go to the IT balance to confirm final weight - don't double check net weight calculation IT will do it for you -