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philip > Mistakes > Flashcards

Mistakes Flashcards

1
Q

most investigations according to gabriel are related to what to tests

A

assays and impurities and IM

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2
Q

Clean and organized work areas are positive because

A

Reduce cross cont
Reduce error
Respect the next analyst

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3
Q

Reagents and solvents exp date

A

Date on manufactured bottle coa

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4
Q

NIR Mistake before login on

To the computer

A

Make sure you are using the right instrument in the instrument selector.

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5
Q

Remember Shannon mistake documention correction on the retain

A

Should read (correct sample ID)

Accidentally hit print with incorrect decimal places

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6
Q

Review pH procedure

A

Calibrate, and check buffers they must be within 0.03.

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7
Q

hplc maintenance sop

A

11360 major minor repairs

moisture check anakyzers

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8
Q

sensitivity injection

A

measure instument response on very low concentations

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9
Q

ANSI stands for

A

American national standard institute

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10
Q

Bill takeaway 2

A

It is what it is

100.0% confidence

Difference between analyst and a good analyst

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11
Q

nPOB1 and nPOB2

A

next generation purified oxycodone base step 1

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12
Q

Micronized is only from

A

athens

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13
Q

Zachary ferrule why does it exist and how to make it?

A

It exist so that the Column attaches with out falling. The fitting must slide freely but not fall.

Twist once. And then tighten and untighten with wrench.

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14
Q

Mural

A

King of sweden swweede landing

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15
Q

nCOB stands for

A

next generation crude oxycodone base

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16
Q

Nothing with data goes in trash

A

Shredder

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17
Q

Types of solutions for ph

A

Storage solutions and filling solutions

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18
Q

Documents to check when receing tankers and what to check on them

A
  • COA
  • BO Lading
  • Wash Certificate must be signed

(Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter of dedication)

Check that they are initial and date and batch from someone from the warehouse

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19
Q

When trying to focus in on the global IM microscope part

A

Use top light and start at 5x

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20
Q

how do you know the tapes need to be reloeaded?

A

you get the pink

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21
Q

Glassware washing 3 steps —- pipettes

A

Acero acid, tap and DI water — tip up, column rinsing wait when the water level is down, tip down on furnaces

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22
Q

Safety always card in and out buttons and exitinguesrs

A

Panic button medical alert buttons

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23
Q

Extra details when washing pipets Shannon

A

Pop 2 pills and leave 3 hours rinsing

Then dry 3 hours tip down

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24
Q

Zach ask questions

A

As i go

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25
oven purge instruccions BEFORE TURNING OFF make sure
turn on pump, open line, slight purge 20 to 25 mg somethings you pay attention if other people are running stuff
26
How to dispose of a reagent
it has a CH sticker - non controlled moved - disposed two boxes on the right - flush the container with water - cross out with a sharpie throw in the trash
27
What to remember about the plug in ph
Plug when not In use unplug when in use
28
get used to calibration decimal and units checking
-
29
Waste inventory spreadsheet zach
Departments EHS waste inventory make sure its in Wilmington
30
COM
crude oxymorphone
31
What is used to decolor powders ?
Loose carbon or encapsulated carbon
32
Production should put the ---- weight on the bag
Tate
33
HM I S
Health materials identification system
34
Dial number emergency
55
35
Where are the stock stds in the safe from?
They buy no USP stds they make theyre own jn athens.
36
IOP stands for
instrument operating procedure
37
Roi stands for
Residue on ignition
38
Whats in the safe?
Retains disposal stock stds
39
Whenever you sign as a witness you share in the --- remember you can
Responsibility remember you can always decline.
40
Micro cal and bulk calibration due
Micro every 3 months bulk every 6
41
Raw materials that are received could be either two things And what do yo do with them after you receive them
Label checks or raw materials in jars with green lids to be tested Whenever they're received they're immediately disposed
42
KF Equation detail you didn't know
ml * KF factor / weight of sample
43
FG acronym
Fine grade
44
0. 04 0. 06 What is that? Bill asked
It means nothing without any units.
45
on the LOP SOP it says about 30 minutes accordig to danielle it should be
NLT then 30 min
46
PM Is what
Preventive maintenance
47
nPHB
next generation purified hydrocodone base
48
Remember I just don't work with APIs I work with ----- Edwin
Narcotics
49
where are the tubes used in comparison
S2-3
50
What is CAPA?
Corrective action preventive action.
51
Audit trails
Are a reconstruction of how the batch came to be Think about training validation was it cleaned.
52
Orion 3 ph Jackie didn't know how to change from mV to ph
Justin had to come and press down.
53
Difference between environmental impact an element
An element is something which can be impacted
54
Danielle NIR out of what range
Always check the calibration range
55
20/20/20vision rule
Use the 20-20-20 rule. Every 20 minutes, take a 20-second break and focus your eyes on something at least 20 feet away.
56
--- g of tolerance , how much for weight cakes
0.3 g 1% Of how much
57
Special detail Shannon taught you about the NIR
Put the sample as soon as you get to the area
58
It its an old tanker lot if wont bring
A COA
59
What is the bill of lading?
Check MFG and disctributor adress this is used to determined reduced or full testing Make sure its legible
60
Chain of custody bill meeting
Always check in and out
61
crude vs next generation
crude is like with impurities next genertaion
62
When doing the balances don't write the ----!!
Units. It's usually included.
63
Appearance EC
Fill in the circles, if it tells you to write it, you should always choose white or white off not both.
64
What would be a considered as metallic particle
Anything silver or shiny.
65
Just remember tepentadol gets
CE
66
The two big balances are called ---
Pan
67
How do i know the tolerances for each balances ? What about the weight set?
SOP fot the olerances. The actual weights change when the weight set changes.
68
raman sample holders
vial holder nose cone (this is used directly against the sample container)
69
according to game stress before cleanup reduces
downtime
70
fLOD procedure
fLOD Halogen moisture Balance training EC 11-28-16 remember on/off button, tare button, open/close button (last 24 hours, this calibration has no print out ) method button to choose the material or product hit enter code button to enter sample info c1 sample a-z letter to switch to alphabet up down arrow c2 batch c3 extra info keep hitting code until I come to the home screen print out and compare to table add sample spread it hit start wet wight is my weight
71
nATA stans for
nxt generation anhydrous thebaine alkaloid
72
when writing a bought mfg chemical write
MFG, lot no
73
Mental conflation. Non routines va non controlled
It is obvious
74
when to accept non routine samples?
SA, PR # or a CoC
75
Noncoformqnces types
Events Deviations Events -(ICMS)
76
Bill meeting When an auditor comes to check all documents what is this called
Audit trail
77
dad detector
diode array detector The main reason for this is that a DAD/PDA can always be set to scan a range of all probable wavelengths, but a single (or multi-wavelength) detector can not.
78
Phone interview
Exited introductions meting new people
79
Mobile phase filters
0.45 micron MP
80
remmebr to fill forrest zach
departmetns --> wilimgnton --> enviromental -->wast inventory departmetns --> wilimgnton --> hazard communication--> sds
81
Retain Shannon mistake weighing
Always make sure it is in the right decimal place.
82
finished product is the only one with ---- retain date eveything else that goes on the ---- gets 1
finished gets 6 year, eveything else in the green lid jar gets 1 year
83
ICMS
Instrument calibration maintenance system Instrument Calibration & Maintenance System (ICMS) is a convenient way to maintain all your records on the equipment, machinery, instrumentation, and very much all of your company assets. Supplied as a separate product or as an integrated part of any Matrix Gemini modules, it holds and reports on any important information. ICMS tracks all your assets, starting from installation, maintenance, repairs, calibration until the disposal of any unusable assets.
84
How to turn off vacuum LOD
Turn off punk first then the valve the release the pressure
85
Where are the frops planted ? And what are they called
Tazmania poppy seeds
86
DOT
Department of transportation
87
Remind yourself of the button to change units in the balances and digits on the pH
-
88
Choose what when choosing NIR results
Measurement done:
89
Excel keep paswrod
For passweod
90
watch for the double negative in the
NAOH tanker
91
Product flow chart
RM->Wet ->Dry->Mill?->Finishing?
92
Spec says <0.10% Your results are 0.0045% how should you report it
0.005% always report something
93
What's the difference between an analyst and good analyst ?
Analyst produces results and a good analyst ask if it makes sense
94
Post it notes 3 bill
Do I understand what they're asking ? Do I owe it? Do I agree?
95
Read well. What about the sample?
Is it dried or wet

philip (20 decks)

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