Synthesis Flashcards
(12 cards)
Dissolving
Aids the reaction by increasing collisions
Filtration
This separates the insoluble solids from liquids to remove the product from the mixture
Crystallisation
This forms crystals from a solution by removing the solvent
Evaporation
This forms a powder from a solution by removing the solvent
Drying
In an oven or desiccator
Removes water left in the product
What are the stages of synthesis
- Deciding which chemicals to use
- Risk assessment
- Mass needed to make a certain mass of product to limit waste
- Select equipment conditions and concentration
- Make product
- Purify product
- Measure the purity by titration to ensure it is suitable for use
Metal + acid
Salt + hydrogen
Acid + metal oxide
Salt + water
Acid + metal hydroxide
Salt + water
Metal Carbonate + acid
Salt + water + co2
Stages of titration
- Add acid to burette and record initial volume
- Measure alkali in volumetric pipette using a pipette filler, add to conical flask
- Add a few drops of indicator
- Slowly add acid to flask until colour change
- Record final volume
To make a titration more accurate
Flask on white tile
Repeat until you get consistent results
Swirl the flask as acid is added
Add acid drop by drop